e-ISSN 2231-8526
ISSN 0128-7680
Mohd Shahrul Nizam Salleh, Roshafima Rasit Ali, Norzila Mohd, Fatahiya Mohamed Tap, Iswaibah Mustafa and Zatil Izzah Tarmizi
Pertanika Journal of Science & Technology, Volume 33, Issue S3, December 2025
DOI: https://doi.org/10.47836/pjst.33.S3.01
Keywords: Composite, full factorial design, injection moulding, polyvinyl alcohol, starch
Published on: 2025-04-24
The combination of polyvinyl alcohol (PVOH) and starch composites leads to the production of biodegradable polymer composites. This polymer compound has good qualities for being used as a biodegradable material, which makes it easier to stop the buildup of synthetic substances made from petroleum. This study is intended to analyse the processability characteristics of PVOH-starch composites using actual injection moulding. The processability study of PVOH-starch found that the compound could be injection moulded. The name tag product (NTP) was used as a product outcome during the injection moulding. The verification of the optimisation was conducted by means of statistical analysis employing full-factorial design methodologies. In short, the statistical results have indicated that optimal processing techniques can contribute to the production of NTP with little volumetric shrinkage (as observed in short-shot scenarios) while maintaining acceptable levels of variability. Finally, the optimum injection moulding process parameters were found at 200°C and a pressure of 90 bar. This is because the NTP was produced at the lowest variation of the NTP’s total weight in this set of parameters.
Antony, J. (2023). 6 - Full factorial designs. In J. Antony (Ed.), Design of experiments for engineers and scientists (3rd ed., pp. 65-87). Elsevier. https://doi.org/https://doi.org/10.1016/B978-0-443-15173-6.00009-3
Bercea, M. (2024). Recent advances in poly(vinyl alcohol)-based hydrogels. Polymers, 16(14), 2021. https://doi.org/10.3390/polym16142021
Chopra, P., Garg, S., & Jana, A. K. (2013). Study on the performance of starch / PVA blend films modified with SiO 2 Nanoparticles. International Journal of Research in Mechanical Engineering & Technology, 3(2), 36-40.
Flores, S., Famá, L., Rojas, A. M., Goyanes, S., & Gerschenson, L. (2007). Physical properties of tapioca-starch edible films: Influence of filmmaking and potassium sorbate. Food Research International, 40(2), 257-265. https://doi.org/https://doi.org/10.1016/j.foodres.2006.02.004
Ghazy, O. A., Nabih, S., Abdel-moneam, Y. K., & Senna, M. M. (2016). Polyvinyl alcohol-modified Pithecellobium Clypearia Benth herbal residue fiber/polypropylene composites. Polymer Composites, 37(1), 915-924. https://doi.org/10.1002/pc
Gülçür, M., Brown, E., Gough, T., & Whiteside, B. (2023). Characterisation of microneedle replication and flow behaviour in ultrasonic micro-injection moulding through design of experiments. Journal of Manufacturing Processes, 102, 513-527. https://doi.org/https://doi.org/10.1016/j.jmapro.2023.07.068
Jagannath, J. H., Nadanasabapathi, S., & Bawa, A. S. (2006). Effect of starch on thermal, mechanical, and barrier properties of low density polyethylene film. Journal of Applied Polymer Science, 99(6), 3355-3364. https://doi.org/https://doi.org/10.1002/app.22358
Jung, J., Park, K., Cho, B., Park, J., & Ryu, S. (2023). Optimization of injection molding process using multi-objective bayesian optimization and constrained generative inverse design networks. Journal of Intelligent Manufacturing, 34(8), 3623-3636. https://doi.org/10.1007/s10845-022-02018-8
Krantz, J., Nieduzak, Z., Kazmer, E., Licata, J., Ferki, O., Gao, P., Sobkowicz, M. J., & Masato, D. (2023). Investigation of pressure-controlled injection molding on the mechanical properties and embodied energy of recycled high-density polyethylene. Sustainable Materials and Technologies, 36, e00651. https://doi.org/https://doi.org/10.1016/j.susmat.2023.e00651
Liou, G.-Y., Su, W.-J., Cheng, F.-J., Chang, C.-H., Tseng, R.-H., Hwang, S.-J., Peng, H.-S., & Chu, H.-Y. (2023). Optimize injection-molding process parameters and build an adaptive process control system based on nozzle pressure profile and clamping force. Polymers, 15(3), 610. https://doi.org/10.3390/polym15030610
Liu, D., Dang, S., Zhang, L., Munsop, K., & Li, X. (2021). Corn starch/polyvinyl alcohol based films incorporated with curcumin-loaded Pickering emulsion for application in intelligent packaging. International Journal of Biological Macromolecules, 188, 974-982. https://doi.org/https://doi.org/10.1016/j.ijbiomac.2021.08.080
Moo-Tun, N. M., Iñiguez-Covarrubias, G., & Valadez-Gonzalez, A. (2020). Assessing the effect of PLA, cellulose microfibers and CaCO3 on the properties of starch-based foams using a factorial design. Polymer Testing, 86, 106482. https://doi.org/https://doi.org/10.1016/j.polymertesting.2020.106482
Othman, N., & Azahari, N. (2011). Thermal properties of polyvinyl alcohol (PVOH)/corn starch blend film. Malaysian Polymer Journal, 6(6), 147-154.
Pan, W., Liang, Q., & Gao, Q. (2022). Preparation of hydroxypropyl starch/polyvinyl alcohol composite nanofibers films and improvement of hydrophobic properties. International Journal of Biological Macromolecules, 223, 1297-1307. https://doi.org/https://doi.org/10.1016/j.ijbiomac.2022.11.114
Ramesh, M. (2016). Kenaf (Hibiscus cannabinus L.) fibre based bio-materials: A review on processing and properties. Progress in Materials Science, 78–79, 1-92. https://doi.org/10.1016/j.pmatsci.2015.11.001
Ray, R., Narayan Das, S., & Das, A. (2021). Mechanical, thermal, moisture absorption and biodegradation behaviour of date palm leaf reinforced PVA/starch hybrid composites. Materials Today: Proceedings, 41, 376-381. https://doi.org/https://doi.org/10.1016/j.matpr.2020.09.564
Sangthongdee, M., Phattarateera, S., & Threepopnatkul, P. (2022). The effect of pregelatinized starch on the properties of poly (vinyl alcohol) film for the water-soluble laundry bag. Chiang Mai Journal of Science, 49(6), 1604-1617. https://doi.org/10.12982/CMJS.2022.096
Shogren, R. L. (1995). Poly(ethylene oxide)-coated granular starch-poly(hydroxybutyrate-co-hydroxyvalerate) composite materials. Journal of Environmental Polymer Degradation, 3(2), 75-80. https://doi.org/10.1007/BF02067483
Siddaramaiah, Raj, B., & Somashekar, R. (2004). Structure–property relation in polyvinyl alcohol/starch composites. Journal of Applied Polymer Science, 91(1), 630-635. https://doi.org/https://doi.org/10.1002/app.13194
Trotta, G., Stampone, B., Fassi, I., & Tricarico, L. (2021). Study of rheological behaviour of polymer melt in micro injection moulding with a miniaturized parallel plate rheometer. Polymer Testing, 96, 107068. https://doi.org/https://doi.org/10.1016/j.polymertesting.2021.107068
Wang, S., Zhang, P., Li, Y., Li, J., Li, X., Yang, J., Ji, M., Li, F., & Zhang, C. (2023). Recent advances and future challenges of the starch-based bio-composites for engineering applications. Carbohydrate Polymers, 307, 120627. https://doi.org/https://doi.org/10.1016/j.carbpol.2023.120627
ISSN 0128-7680
e-ISSN 2231-8526